Reduced to Hierarchy: Carbon Filament-Supported Mixed Metal Oxide Nanoparticles

G. V. Manohara, Andrew Whiting, H. Chris Greenwell

Research output: Contribution to journalArticlepeer-review

2 Citations (Scopus)
20 Downloads (Pure)


We describe a one-pot synthesis method for carbon filament-supported mixed metal oxide nanoparticles. The thermal intracrystalline reaction of adamantanecarboxylate ions confined inside interlayer galleries of layered double hydroxide materials under a reducing atmosphere (H2) leads to carbon filaments forming in situ within the material. Raman spectroscopy and combined microscopy techniques show the formation of hybrid organic-inorganic carbon filaments with the mixed metal oxide particles interleaved.

Original languageEnglish
Pages (from-to)20230-20236
Number of pages7
JournalACS Omega
Issue number23
Early online date20 Nov 2019
Publication statusPublished - 3 Dec 2019


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