Pseudo-polymorphism in the toluene solvate of p-tert-butylcalix[5]arene: Structural and gas sorption investigation

Scott J. Dalgarno; Praveen K. Thallapally; Jian Tian; Jerry L. Atwood

doi:10.1039/b809457h

Pseudo-polymorphism in the toluene solvate of p-tert-butylcalix[5]arene: Structural and gas sorption investigation

Scott J. Dalgarno, Praveen K. Thallapally, Jian Tian, Jerry L. Atwood

School of Engineering & Physical Sciences

Research output: Contribution to journal › Article › peer-review

5 Citations (Scopus)

Abstract

Crystallisation of the host molecule p-tert-butylcalix[5]arene from toluene affords three pseudo-polymorphs, two of which can be isolated on a large scale and used to form 'frustrated' organic solids that are capable of gas sorption. The structures of these three polymorphs are compared, and the gas sorption capabilities of the two phases that can be isolated in bulk form are described. © The Royal Society of Chemistry and the Centre National de la Recherche Scientifique 2008.

Original language	English
Pages (from-to)	2095-2099
Number of pages	5
Journal	New Journal of Chemistry
Volume	32
Issue number	12
DOIs	https://doi.org/10.1039/b809457h
Publication status	Published - 2008

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AB - Crystallisation of the host molecule p-tert-butylcalix[5]arene from toluene affords three pseudo-polymorphs, two of which can be isolated on a large scale and used to form 'frustrated' organic solids that are capable of gas sorption. The structures of these three polymorphs are compared, and the gas sorption capabilities of the two phases that can be isolated in bulk form are described. © The Royal Society of Chemistry and the Centre National de la Recherche Scientifique 2008.

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Pseudo-polymorphism in the toluene solvate of p-tert-butylcalix[5]arene: Structural and gas sorption investigation

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