Non-destructive thickness measurement of thermal barrier coatings using terahertz radiation

Luis Isern, Andrew J. Waddie, Christine Chalk, Andrew J. Moore, John R. Nicholls

Research output: Contribution to journalArticlepeer-review

Abstract

A non-destructive thickness measurement technique based on terahertz (THz) reflectivity was successfully deployed to interrogate 7 wt.% yttria-stabilised zirconia thermal barrier coatings (TBCs) produced by electron-beam physical vapour deposition (EB-PVD). The THz technique was shown to produce accurate thickness maps for different samples with a resolution of 1 × 1 mm over a surface of 65 × 20 mm that were compared with direct examination of key cross-sections. All thickness measurements on different samples were calculated using a single value of refractive index. Small defects characteristic of EB-PVD, such as “carrot growths” and variations on column inclination, were evaluated and did not produce significant variations in the refractive index of the TBC. Moreover, the thickness maps correctly display thickness variations that are a consequence of the point-source nature of EB-PVD evaporation. In summary, this paper demonstrates the technique can be successfully deployed on large surfaces, and across different coatings of the same material produced under the same deposition conditions. It is shown that a single n value is required to map the thickness distribution for all samples. This combination of qualities indicates the potential of the technique for in-line control of TBC manufacture.

Original languageEnglish
JournalEmergent Materials
Early online date6 Aug 2021
DOIs
Publication statusE-pub ahead of print - 6 Aug 2021

Keywords

  • Electron-beam physical vapour deposition
  • Optical properties
  • Terahertz imaging
  • Thermal barrier coatings

ASJC Scopus subject areas

  • Biomaterials
  • Renewable Energy, Sustainability and the Environment
  • Waste Management and Disposal
  • Ceramics and Composites

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