Crystal structure of 1,1'-bis[1,7-dicarba-closo-dodecaborane(11)]

Lisa Elrick; Georgina Margaret Rosair; Alan Jeffrey Welch

doi:10.1107/S1600536814022132

Crystal structure of 1,1'-bis[1,7-dicarba-closo-dodecaborane(11)]

Lisa Elrick, Georgina Margaret Rosair, Alan Jeffrey Welch

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Abstract

In the title compound, C4H22B20, the two {1,7-closo-C2B10H11} cages are linked across a centre of inversion with C–C = 1.5401(16) Å. The position of the second non-linking cage C atom was established unambiguously by geometric and crystallographic methods and there is no evidence of C/B disorder.

Original language	English
Pages (from-to)	376-378
Number of pages	3
Journal	Acta Crystallographica Section E: Structure Reports Online
Volume	70
Issue number	11
DOIs	https://doi.org/10.1107/S1600536814022132
Publication status	Published - Nov 2014

Keywords

Crystal structure
carboranes
closo-dodecaborane(11)

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10.1107/S1600536814022132

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title = "Crystal structure of 1,1'-bis[1,7-dicarba-closo-dodecaborane(11)]",

abstract = "In the title compound, C4H22B20, the two \{1,7-closo-C2B10H11\} cages are linked across a centre of inversion with C–C = 1.5401(16) {\AA}. The position of the second non-linking cage C atom was established unambiguously by geometric and crystallographic methods and there is no evidence of C/B disorder.",

keywords = "Crystal structure, carboranes, closo-dodecaborane(11)",

author = "Lisa Elrick and Rosair, \{Georgina Margaret\} and Welch, \{Alan Jeffrey\}",

year = "2014",

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doi = "10.1107/S1600536814022132",

language = "English",

volume = "70",

pages = "376--378",

journal = "Acta Crystallographica Section E: Structure Reports Online",

issn = "1600-5368",

publisher = "International Union of Crystallography",

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T1 - Crystal structure of 1,1'-bis[1,7-dicarba-closo-dodecaborane(11)]

AU - Elrick, Lisa

AU - Rosair, Georgina Margaret

AU - Welch, Alan Jeffrey

PY - 2014/11

Y1 - 2014/11

N2 - In the title compound, C4H22B20, the two {1,7-closo-C2B10H11} cages are linked across a centre of inversion with C–C = 1.5401(16) Å. The position of the second non-linking cage C atom was established unambiguously by geometric and crystallographic methods and there is no evidence of C/B disorder.

AB - In the title compound, C4H22B20, the two {1,7-closo-C2B10H11} cages are linked across a centre of inversion with C–C = 1.5401(16) Å. The position of the second non-linking cage C atom was established unambiguously by geometric and crystallographic methods and there is no evidence of C/B disorder.

KW - Crystal structure

KW - carboranes

KW - closo-dodecaborane(11)

U2 - 10.1107/S1600536814022132

DO - 10.1107/S1600536814022132

M3 - Article

C2 - 25484750

SN - 1600-5368

VL - 70

SP - 376

EP - 378

JO - Acta Crystallographica Section E: Structure Reports Online

JF - Acta Crystallographica Section E: Structure Reports Online

IS - 11

ER -

Crystal structure of 1,1'-bis[1,7-dicarba-closo-dodecaborane(11)]

Abstract

Keywords

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