A high temperature cell for simultaneous electrical resistance and neutron diffraction measurements

T. E. Engin; A. V. Powell; R. Haynes; M. A H Chowdhury; C. M. Goodway; R. Done; O. Kirichek; S. Hull

doi:10.1063/1.2979011

A high temperature cell for simultaneous electrical resistance and neutron diffraction measurements

T. E. Engin, A. V. Powell, R. Haynes, M. A H Chowdhury, C. M. Goodway, R. Done, O. Kirichek, S. Hull

School of Engineering & Physical Sciences

Research output: Contribution to journal › Article › peer-review

12 Citations (Scopus)

Abstract

An in situ cell that allows the electrical resistance of a sample pellet to be measured while performing neutron diffraction experiments has been developed at the ISIS pulsed neutron source. The sample is held between two spring loaded platinum electrodes embedded in a boron nitride clamp assembly with the resistance measured using the four-probe method. An outer quartz glass jacket allows the atmosphere within the sample enclosure to be controlled, and the entire device can be accommodated within a standard ISIS neutron furnace for measurements at temperatures up to 1270 K. The operation of this cell is illustrated using data for the structural, magnetic, and electrical properties of chalcopyrite CuFeS2 collected over the temperature range of 398-873 K on the Polaris powder diffractometer at ISIS. © 2008 American Institute of Physics.

Original language	English
Article number	095104
Journal	Review of Scientific Instruments
Volume	79
Issue number	9
DOIs	https://doi.org/10.1063/1.2979011
Publication status	Published - 2008

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10.1063/1.2979011

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title = "A high temperature cell for simultaneous electrical resistance and neutron diffraction measurements",

abstract = "An in situ cell that allows the electrical resistance of a sample pellet to be measured while performing neutron diffraction experiments has been developed at the ISIS pulsed neutron source. The sample is held between two spring loaded platinum electrodes embedded in a boron nitride clamp assembly with the resistance measured using the four-probe method. An outer quartz glass jacket allows the atmosphere within the sample enclosure to be controlled, and the entire device can be accommodated within a standard ISIS neutron furnace for measurements at temperatures up to 1270 K. The operation of this cell is illustrated using data for the structural, magnetic, and electrical properties of chalcopyrite CuFeS2 collected over the temperature range of 398-873 K on the Polaris powder diffractometer at ISIS. {\textcopyright} 2008 American Institute of Physics.",

author = "Engin, {T. E.} and Powell, {A. V.} and R. Haynes and Chowdhury, {M. A H} and Goodway, {C. M.} and R. Done and O. Kirichek and S. Hull",

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AU - Engin, T. E.

AU - Powell, A. V.

AU - Haynes, R.

AU - Chowdhury, M. A H

AU - Goodway, C. M.

AU - Done, R.

AU - Kirichek, O.

AU - Hull, S.

PY - 2008

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N2 - An in situ cell that allows the electrical resistance of a sample pellet to be measured while performing neutron diffraction experiments has been developed at the ISIS pulsed neutron source. The sample is held between two spring loaded platinum electrodes embedded in a boron nitride clamp assembly with the resistance measured using the four-probe method. An outer quartz glass jacket allows the atmosphere within the sample enclosure to be controlled, and the entire device can be accommodated within a standard ISIS neutron furnace for measurements at temperatures up to 1270 K. The operation of this cell is illustrated using data for the structural, magnetic, and electrical properties of chalcopyrite CuFeS2 collected over the temperature range of 398-873 K on the Polaris powder diffractometer at ISIS. © 2008 American Institute of Physics.

AB - An in situ cell that allows the electrical resistance of a sample pellet to be measured while performing neutron diffraction experiments has been developed at the ISIS pulsed neutron source. The sample is held between two spring loaded platinum electrodes embedded in a boron nitride clamp assembly with the resistance measured using the four-probe method. An outer quartz glass jacket allows the atmosphere within the sample enclosure to be controlled, and the entire device can be accommodated within a standard ISIS neutron furnace for measurements at temperatures up to 1270 K. The operation of this cell is illustrated using data for the structural, magnetic, and electrical properties of chalcopyrite CuFeS2 collected over the temperature range of 398-873 K on the Polaris powder diffractometer at ISIS. © 2008 American Institute of Physics.

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VL - 79

JO - Review of Scientific Instruments

JF - Review of Scientific Instruments

IS - 9

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ER -

A high temperature cell for simultaneous electrical resistance and neutron diffraction measurements

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