1,4,8,11 -Tetraazacyclotetradecane antimony(III) sulfide

R. J E Lees; Anthony V. Powell; David J. Watkin; Ann M. Chippindale

doi:10.1107/S010827010605044X

1,4,8,11 -Tetraazacyclotetradecane antimony(III) sulfide

R. J E Lees
, Anthony V. Powell
, David J. Watkin
, Ann M. Chippindale

School of Engineering & Physical Sciences

Research output: Contribution to journal › Article › peer-review

11 Citations (Scopus)

Abstract

Poly[1,4,8,11-tetraazacyclotetradecane(2+) [hepta-µ-sulfido- trisulfidohexaantimony(III)]], {(C₁₀H₂₆N ₄)[Sb₆S₁₀]}_n, consists of novel [Sb₆S₁₀]^2- layers containing Sb ₂S₂, Sb₄S₄ and Sb₇S ₇ hetero-rings, which are separated by macrocyclic amine molecules. The macrocyclic amine molecules are disordered over two crystallographically distinct positions and are diprotonated in order to balance the charge of the anionic layers. © 2007 International Union of Crystallography.

Original language	English
Pages (from-to)	m27-m29
Journal	Acta Crystallographica Section C: Crystal Structure Communications
Volume	63
Issue number	1
DOIs	https://doi.org/10.1107/S010827010605044X
Publication status	Published - 2007

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title = "1,4,8,11 -Tetraazacyclotetradecane antimony(III) sulfide",

abstract = "Poly[1,4,8,11-tetraazacyclotetradecane(2+) [hepta-µ-sulfido- trisulfidohexaantimony(III)]], \{(C10H26N 4)[Sb6S10]\}n, consists of novel [Sb6S10]2- layers containing Sb 2S2, Sb4S4 and Sb7S 7 hetero-rings, which are separated by macrocyclic amine molecules. The macrocyclic amine molecules are disordered over two crystallographically distinct positions and are diprotonated in order to balance the charge of the anionic layers. {\textcopyright} 2007 International Union of Crystallography.",

author = "Lees, \{R. J E\} and Powell, \{Anthony V.\} and Watkin, \{David J.\} and Chippindale, \{Ann M.\}",

year = "2007",

doi = "10.1107/S010827010605044X",

language = "English",

volume = "63",

pages = "m27--m29",

journal = "Acta Crystallographica Section C: Crystal Structure Communications",

issn = "0108-2701",

publisher = "International Union of Crystallography",

number = "1",

}

TY - JOUR

T1 - 1,4,8,11 -Tetraazacyclotetradecane antimony(III) sulfide

AU - Lees, R. J E

AU - Powell, Anthony V.

AU - Watkin, David J.

AU - Chippindale, Ann M.

PY - 2007

Y1 - 2007

N2 - Poly[1,4,8,11-tetraazacyclotetradecane(2+) [hepta-µ-sulfido- trisulfidohexaantimony(III)]], {(C10H26N 4)[Sb6S10]}n, consists of novel [Sb6S10]2- layers containing Sb 2S2, Sb4S4 and Sb7S 7 hetero-rings, which are separated by macrocyclic amine molecules. The macrocyclic amine molecules are disordered over two crystallographically distinct positions and are diprotonated in order to balance the charge of the anionic layers. © 2007 International Union of Crystallography.

AB - Poly[1,4,8,11-tetraazacyclotetradecane(2+) [hepta-µ-sulfido- trisulfidohexaantimony(III)]], {(C10H26N 4)[Sb6S10]}n, consists of novel [Sb6S10]2- layers containing Sb 2S2, Sb4S4 and Sb7S 7 hetero-rings, which are separated by macrocyclic amine molecules. The macrocyclic amine molecules are disordered over two crystallographically distinct positions and are diprotonated in order to balance the charge of the anionic layers. © 2007 International Union of Crystallography.

UR - https://www.scopus.com/pages/publications/33846093922

U2 - 10.1107/S010827010605044X

DO - 10.1107/S010827010605044X

M3 - Article

SN - 0108-2701

VL - 63

SP - m27-m29

JO - Acta Crystallographica Section C: Crystal Structure Communications

JF - Acta Crystallographica Section C: Crystal Structure Communications

IS - 1

ER -

1,4,8,11 -Tetraazacyclotetradecane antimony(III) sulfide

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